Alternative to lead acetate in sugar cane and sugar beet analyses

Number

135-EN

Section

General Section

Use

Sector

Manufacture of food products
Scientific research and development

Function

Solids separation (precipitating) agent

Process

Manual activities involving hand contact

Product category

Processing aids such as pH-regulators, flocculants, percipitant, neutalization agents
laboratory chemicals

Application

analysis of sugar cane and sugar beet

Abstract

Lead acetate can be replaced by aluminium sulphate in analysing sugar cane and sugar beet. Using alternative analytical methods that do not involve lead acetate is also possible.

Substituted substances

Lead acetate, basic

CAS No. 1335-32-6 EC No. 215-630-3 Index No. 082-007-00-9

Chemical group

Lead compounds; carboxylic acid salts

Classification: hazard statements

H351 Suspected of causing cancer
H360Df May damage the unborn child. Suspected of damaging fertility
H373 May cause damage to organs through prolonged or repeated exposure
H400 Very toxic to aquatic life
H410 Very toxic to aquatic life with long lasting effects

Alternative Substances

Aluminium sulphate

CAS No. 10043-01-3 EC No. 233-135-0 Index No.

Chemical group

Aluminum compounds; sulfates

Other adverse effects

Aluminium is included in the Substance database according to SUBSPORT screening criteri ( SDSC)  as neurotoxic ( Vela level 4).

Diatomite

CAS No. 61790-53-2 EC No. Index No.

Chemical group

Silicas

Reliability of information

Internet information: data are from an internet document and only a basic and partial evaluation could be performed

Reason substitution

skin/respiratory sensitizing
ecotoxicity
other toxic effects

Other type of alternative

Infrared polarimetry

Hazard Assessment

Substance to be substituted: Lead acetate basic may damage the unborn child and is suspected of damaging fertility, is very toxic to aquatic life, is very toxic to aquatic life with long lasting effects, is harmful if swallowed, is harmful if inhaled and may cause damage to organs through prolonged or repeated exposure. Alternative substances: Aluminium sulphate and diatomite ha no harmonised classification according to Annex VI of Regulation (EC) No 1272/2008 (CLP Regulation).

Description of Substitution

Lead acetate basic is used as clarifying agent in the polarisation method (visible light range) for analysing sucrose in sugar cane and beet juice. As it is reprotoxic and a suspected carcinogen it should be substituted. It can be replaced by aluminium sulphate. In the case of very turbid juices, diatomite may be used to improve clarity. Avoiding lead acetate may be also achieved by choosing a different type of analytical method: filtering the juice with diatomite and then using a polarimeter at 825 nm or using infrared spectrophotometry. All these methods represent alterations of the official method in France and therefore need to be validated.

Case/substitution evaluation

Aluminium sulphate and diatomite can be used to replace more hazardous lead acetate. If the diatomite is of the flux-calcined type it may contain high levels of crystalline silica, a carcinogen. The consequences of the use of diatomite, which may contain carcinogenic substances, cannot be foreseen here, so further research is required.

State of implementation

In use

Date and place of implementation

France

Availability ofAlternative

Alternative available on the market

Type of information supplier

Authority

Contact

INRS - INSTITUT NATIONAL DE RECHERCHE ET DE SÉCURITÉ pour la prévention des accidents du travail et des maladies professionnelle, France, http://www.inrs.fr www.inrs.fr

Type of publication and availability

Fact sheet

Publication source: author, company, institute, year

The Fact sheet was developed by CNAMTS and INRS, France and published by INRS in 2011.

Publication source

Type of publication and availability

http://www.inrs.fr/accueil/produits/mediatheque/doc/publications.html?refINRS=FAS%2015

Date, reviewed

December 11, 2020