Substitution of Chloroform with 1-Bromo-3-chloropropane in RNA-isolation.

Number

071-EN

Section

General Section

Use

Sector

Scientific research and development

Function

Solvent

Process

Manual activities involving hand contact

Product category

laboratory chemicals

Application

Seperating RNA from DNA and Proteins

Abstract

Chloroform is commonly used in a method to isolate RNA from DNA and proteins. Since chloroform is a neurotoxicant, an endocrine disruptor and possibly also a carcinogen, substitution of the substance is advantageous from a workers' safety perspective. It was found that 1-Bromo-3-chloropropane (BCP) could work as a fully functional substitute for chloroform without any changes in the experimental process.

Substituted substances

Chloroform

CAS No. 67-66-3 EC No. 200-663-8 Index No. 602-006-00-4

Chemical group

Chloroalkanes

Classification: hazard statements

H351 Suspected of causing cancer
H361d Suspected of damaging the unborn child
H331 Toxic if inhaled
H302 Harmful if swallowed
H372 Causes damage to organs through prolonged or repeated exposure
H315 Causes skin irritation
H319 Causes serious eye irritation

Other adverse effects

The substance is: 2B carcinogen (IARC),  as listed in the Substance Database according to SUBSPORT Screening Criteria (SDSC).

Alternative Substances

1-Bromo-3-chloropropane

CAS No. 109-70-6 EC No. 203-697-1 Index No.

Chemical group

Halocarbons

Reliability of information

Evidence of implementation: there is evidence that the solution was implemented and in use at time of publication

Reason substitution

CMR
skin/respiratory sensitizing
other toxic effects

Hazard Assessment

Substance to be substituted: Chloroform is a Substance of very high concern and is included on the REACH restriction list, according to Article 73 of Regulation (EG) No. 1907/2006(REACH Regulation). Alternative substance: 1-Bromo-3-chloropropane is possibly carcinogenic to humans (Group 2B), according to the IARC Monographs. » Check the Substance Database according to SUBSPORTplus Screening Criteria (SDSC)

Description of Substitution

In phenol-chloroform extraction RNA is separated from DNA and proteins via a 2-step procedure. The same procedure can also be used to separate DNA or proteins from other compounds. Chloroform is used in the first step where a mixture of chloroform and phenol is mixed with an aqueous solution of the sample containing DNA, RNA and proteins. The combined mixture is then centrifuged, which results in one organic phase and one inorganic phase. The inorganic phase, containing both nucleic acids, is found on top of the vessel allowing it to be extracted. The organic phase, mainly consisting of chloroform will be at the bottom. This phase will contain the proteins of the mixture. DNA can then be separated from RNA in a further step using 2-propanol or ethanol. The substitution of chloroform with BCP does not include any changes in the experimental process. BCP is a less hazardous solvent than chloroform which results in safer working place conditions mainly for the laboratory assistant.

Case/substitution evaluation

The alternative is a less hazardous substance than chloroform, which is of advantage mainly for the laboratory personnel. However, the alternative should be handled carefully, because it is listed in the Substance Database according to SUBSPORT Screening Criteria (SDSC) as well. But in the future this substance should be substituted too because of it risks.

State of implementation

Full capacity

Date and place of implementation

01.09.2010 in Sweden

Enterprise using the alternative

www.sahlgrenska.se

Availability ofAlternative

Fully available.

Producer/Provider

http://www.appliedbiosystems.com/absite/us/en/home.html

Type of information supplier

Research

Date, reviewed

December 11, 2020